3--N-methylamino>-1-methylpiperidine

Base Information

Chemical Name:3--N-methylamino>-1-methylpiperidine
CAS No.:144243-36-7
Molecular Formula:C₁₅H₂₀Cl₂N₂O
Molecular Weight:315.243
Hs Code.:

3-<N-<2-(3,4-dichlorophenyl)acetyl>-N-methylamino>-1-methylpiperidine

Synonyms:3--N-methylamino>-1-methylpiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--N-methylamino>-1-methylpiperidine

Chemical Property:

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Technology Process of 3--N-methylamino>-1-methylpiperidine

There total 7 articles about 3--N-methylamino>-1-methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5807-30-7
3,4-dichlorophenyl acetic acid

: 4606-66-0,1312663-12-9,1354007-31-0
3-(methylamino)-1-methylpiperidine

: 144243-36-7
3--N-methylamino>-1-methylpiperidine

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/jm00101a011

Reference yield:

: 6859-99-0
3-hydroxypiperazine

: 144243-36-7
3--N-methylamino>-1-methylpiperidine

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / aq. NaHCO₃ / 48 h / Ambient temperature

2: 96 percent / Et₃N / tetrahydrofuran / 1 h / Ambient temperature

3: 98 percent / NaN₃ / dimethylformamide / 48 h / 70 °C

4: 69 percent / H₂ / 10percent Pd/C / acetic acid; methanol / 24 h / 2585.7 Torr / Ambient temperature

5: 100 percent / Heating

6: LiAlH₄ / tetrahydrofuran / 4 h / Heating

7: 73 percent / DCC / CH₂Cl₂ / 0.17 h / Ambient temperature

With lithium aluminium tetrahydride; sodium azide; hydrogen; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00101a011

Reference yield:

: 129888-61-5
3-Azido-1-(tert-butoxycarbonyl)piperidine

: 144243-36-7
3--N-methylamino>-1-methylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / H₂ / 10percent Pd/C / acetic acid; methanol / 24 h / 2585.7 Torr / Ambient temperature

2: 100 percent / Heating

3: LiAlH₄ / tetrahydrofuran / 4 h / Heating

4: 73 percent / DCC / CH₂Cl₂ / 0.17 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1021/jm00101a011