benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether

Base Information

• Chemical Name: benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether
• CAS No.: 87678-21-5
• Molecular Formula: C₁₉H₃₀O₄
• Molecular Weight: 322.445

Synonyms:benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether

Chemical Property of benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether

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Technology Process of benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether

There total 38 articles about benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzyl bromide (100-39-0) + 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butan-1-ol (87678-20-4) → benzyl 2(R)-<5(R)-<(methoxymethoxy)methyl>-3(R)-methyl-2(R)-tetrahydrofuryl>butyl ether (87678-21-5)

Guidance literature:

With potassium hydride; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1021/jo00174a008

Reference yield: 97.0%

benzyl bromide (100-39-0) + 2(S)-(5(S)-(methoxymethylenoxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butan-1-ol (84911-66-0,84984-97-4,87678-20-4) → benzyl 2(S)-<5(S)-(methoxymethylenoxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl>butyl ether (84911-68-2,84984-98-5,87678-21-5)

Guidance literature:

With potassium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/ja00345a055

Reference yield: 91.0%

benzyl bromide (100-39-0) + 2(R)-(5(S)-(methoxymethylenoxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butan-1-ol (84911-66-0,84984-97-4,87678-20-4) → benzyl 2(R)-(5(S)-(methoxymethylenoxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butyl ether (84911-68-2,84984-98-5,87678-21-5)

Guidance literature:

With potassium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/ja00345a055

upstream raw materials:

benzyl bromide

2(S)-(5(S)-(methoxymethylenoxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butan-1-ol

2-methyl-2,3-O-(1-methylethylidene)-D-ribonic acid γ-lactone

2-C-methyl-D-ribono-1,4-lactone

Downstream raw materials:

benzyl 2(S)-(5(S)-(hydroxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butyl ether

benzyl 2(R)-(5(S)-carbomethoxy-3(S)-methyl-2(S)-tetrahydrofuryl)butyl ether

(2S,4S,5S)-5-((R)-1-Benzyloxymethyl-propyl)-4-methyl-tetrahydro-furan-2-carboxylic acid

benzyl 2(R)-(5(S)-(hydroxymethyl)-3(S)-methyl-2(S)-tetrahydrofuryl)butyl ether

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