5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

Base Information

Chemical Name:5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole
CAS No.:1268675-68-8
Molecular Formula:C₂₅H₂₀Cl₂N₆
Molecular Weight:475.38
Hs Code.:

Synonyms:5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

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Chemical Property of 5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

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Technology Process of 5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

There total 10 articles about 5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268675-69-9
1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazole-4-nitrile

: 1268675-68-8
5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

Guidance literature:: With sodium azide; diethylaluminium chloride; In toluene; at 0 - 20 ℃; for 3h;

Reference yield:

: 1268682-32-1
N-(5-chloro-2-methyl-phenyl)-3,4-dimethyl-benzamidine

: 1268675-68-8
5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrogencarbonate / water; tetrahydrofuran / 12 h / 20 °C

2.1: toluene-4-sulfonic acid / toluene / 12 h / 60 °C

3.1: N-Bromosuccinimide / acetonitrile / 16 h / 20 °C

4.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 6 h / 85 °C / Inert atmosphere

5.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 4.5 h / 20 - 60 °C

6.1: pyridine; di-tert-butyl dicarbonate / 1,4-dioxane / 0.25 h / 20 °C

6.2: 20 h / 40 °C

7.1: trifluoromethylsulfonic anhydride; triethylamine / dichloromethane / 0.25 h / 0 - 20 °C

8.1: sodium azide; diethylaluminium chloride / toluene / 3 h / 0 - 20 °C

With pyridine; potassium phosphate; N-Bromosuccinimide; sodium azide; lithium hydroxide monohydrate; trifluoromethylsulfonic anhydride; di-tert-butyl dicarbonate; water; diethylaluminium chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 95-79-4
5-chloro-2-methyl-benzenamine

: 1268675-68-8
5-[1-(5-chloro-2-methyl-phenyl)-5-(3-chloro-phenyl)-2-(3,4-dimethyl-phenyl)-1H-imidazol-4-yl]-tetrazole

Guidance literature:: Multi-step reaction with 9 steps

1.1: trimethylaluminum / toluene / 0 - 20 °C

1.2: 20 h / 80 °C

2.1: sodium hydrogencarbonate / water; tetrahydrofuran / 12 h / 20 °C

3.1: toluene-4-sulfonic acid / toluene / 12 h / 60 °C

4.1: N-Bromosuccinimide / acetonitrile / 16 h / 20 °C

5.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 6 h / 85 °C / Inert atmosphere

6.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 4.5 h / 20 - 60 °C

7.1: pyridine; di-tert-butyl dicarbonate / 1,4-dioxane / 0.25 h / 20 °C

7.2: 20 h / 40 °C

8.1: trifluoromethylsulfonic anhydride; triethylamine / dichloromethane / 0.25 h / 0 - 20 °C

9.1: sodium azide; diethylaluminium chloride / toluene / 3 h / 0 - 20 °C

With pyridine; potassium phosphate; N-Bromosuccinimide; sodium azide; lithium hydroxide monohydrate; trifluoromethylsulfonic anhydride; di-tert-butyl dicarbonate; water; trimethylaluminum; diethylaluminium chloride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;