7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

Base Information

Chemical Name:7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine
CAS No.:1254940-13-0
Molecular Formula:C₁₆H₁₆N₆OS
Molecular Weight:340.409
Hs Code.:

Synonyms:7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

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Chemical Property of 7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

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Technology Process of 7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

There total 6 articles about 7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1254940-03-8
1,5-dimethyl-3-phenyl-7,8-dihydro-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine-7-thione

: 1254940-13-0
7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; acetonitrile; for 4h; Reflux;
DOI:10.3184/030823410X520778

Reference yield:

: 74-96-4
ethyl bromide

: C₁₄H₁₂N₆OS

: 1254940-13-0
7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; acetonitrile; for 4h; Heating;
DOI:10.1134/S1068162015020077

Reference yield:

: 1254940-00-5
1,5-dimethyl-7-hydrazino-3-phenyl-1H-pyrimido[4,5-e][1,3,4]oxadiazine

: 1254940-13-0
7-(ethylsulfanyl)-1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 6 h / Reflux

2: triethylamine / acetonitrile; N,N-dimethyl-formamide / 4 h / Heating

With pyridine; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1134/S1068162015020077