Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2)

Base Information

• Chemical Name: Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2)
• CAS No.: 144718-36-5
• Molecular Formula: C₅₂H₅₆Ge₂N₂P₂Pt
• Molecular Weight: 1111.24
• Mol file: 144718-36-5.mol

Synonyms:Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2)

Chemical Property of Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2)

There total 1 articles about Pt(P(C₆H₅)3)2(C₅H₅N)2((CH₃)2GeC₂H₄Ge(CH₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{Pt(P(C6H5)3)2(Ge(CH3)2CH2CH2Ge(CH3)2)} → Pt(P(C6H5)3)2(C5H5N)2((CH3)2GeC2H4Ge(CH3)2) (144718-36-5)

Guidance literature:

With pyridine; heated for 4 h at 100°C under Ar; excess pyridine removed under reduced pressure (E-2 mmHg), detected by NMR;

DOI:10.1016/S0020-1693(00)92390-9

Reference yield: 98.0%

Pt(P(C6H5)3)2(C5H5N)2((CH3)2GeC2H4Ge(CH3)2) (144718-36-5) → bis(triphenylphosphine)platinum(II) dichloride (10199-34-5,14056-88-3,15604-36-1) + 1,2-bis(chlorodimethylgermyl)ethane (63746-65-6)

Guidance literature:

With hydrogenchloride; In diethyl ether; benzene; (N2 or Ar), 20°C, HCl in Et2O used; Pt-compd. removed by filtration, Ge-compd. isolated by crystn. from pentane (soln. concd. under 10 mmHg, pentane added) or detected by GC, NMR;

DOI:10.1016/S0020-1693(00)92390-9

Downstream raw materials:

bis(triphenylphosphine)platinum(II) dichloride

1,2-bis(chlorodimethylgermyl)ethane