C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

Base Information

Chemical Name:C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾
CAS No.:1185947-26-5
Molecular Formula:C₅₇H₆₇ClN₇O₁₁
Molecular Weight:1061.65
Hs Code.:

C<sub>57</sub>H<sub>67</sub>ClN<sub>7</sub>O<sub>11</sub><sup>(1+)</sup>

Synonyms:C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

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Chemical Property of C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

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Technology Process of C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

There total 9 articles about C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 41175-50-2
8-hydroxyjulolidine

: 945225-35-4
[(2-{(2-[2-bis(methoxycarbonylmethyl)amino-4-chlorophenoxy]-7-azidooctan-2-yl)oxy}-4-formylphenyl)(methoxycarbonylmethyl)amino]acetic acid methyl ester

: 1185947-26-5
C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

Guidance literature:: 8-hydroxyjulolidine; [(2-{(2-[2-bis(methoxycarbonylmethyl)amino-4-chlorophenoxy]-7-azidooctan-2-yl)oxy}-4-formylphenyl)(methoxycarbonylmethyl)amino]acetic acid methyl ester; With toluene-4-sulfonic acid; In propionic acid; for 18h;

With chloranil; In dichloromethane; propionic acid; for 4h;
DOI:10.1021/ja304018d

Reference yield:

: 945225-32-1
[(2-{(2-[2-bis(methoxycarbonylmethyl)amino-4-chlorophenoxy]oct-7-en-2-yl)oxy}phenyl)(methoxycarbonylmethyl)amino]acetic acid methyl ester

: 1185947-26-5
C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate; N,N-dimethyl-formamide / 20.5 h / 20 - 45 °C

2.1: hydrogen bromide / dichloromethane; acetic acid / 1 h / 20 °C

3.1: sodium azide / N,N-dimethyl-formamide / 2 h / 100 °C

4.1: toluene-4-sulfonic acid / propionic acid / 18 h

4.2: 4 h

With sodium azide; hydrogen bromide; toluene-4-sulfonic acid; N,N-dimethyl-formamide; trichlorophosphate; In dichloromethane; acetic acid; propionic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja304018d

Reference yield:

: 89-64-5
p-chloro-o-nitrophenol

: 1185947-26-5
C₅₇H₆₇ClN₇O₁₁⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium hydroxide / water; dichloromethane

2.1: N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere

3.1: tin(II) chloride dihdyrate; hydrogenchloride / water; ethanol / 1.5 h / 78 °C

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / Reflux

5.1: trichlorophosphate; N,N-dimethyl-formamide / 20.5 h / 20 - 45 °C

6.1: hydrogen bromide / dichloromethane; acetic acid / 1 h / 20 °C

7.1: sodium azide / N,N-dimethyl-formamide / 2 h / 100 °C

8.1: toluene-4-sulfonic acid / propionic acid / 18 h

8.2: 4 h

With hydrogenchloride; sodium azide; tin(II) chloride dihdyrate; hydrogen bromide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; trichlorophosphate; In ethanol; dichloromethane; water; acetic acid; propionic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja304018d