Technology Process of C20H38O5Si
There total 5 articles about C20H38O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethyl acetate;
for 2h;
Inert atmosphere;
DOI:10.1021/jm201685h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 1 h / -70 °C
1.2: -70 - 20 °C
2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 40 °C
3.1: palladium on activated charcoal; hydrogen / ethyl acetate / 2 h / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium on activated charcoal; hydrogen; lithium diisopropyl amide;
In
tetrahydrofuran; n-heptane; dichloromethane; ethylbenzene; ethyl acetate;
DOI:10.1021/jm201685h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 40 °C
2: palladium on activated charcoal; hydrogen / ethyl acetate / 2 h / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium on activated charcoal; hydrogen;
In
dichloromethane; ethyl acetate;
DOI:10.1021/jm201685h
