2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide

Base Information

• Chemical Name: 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide
• CAS No.: 136667-97-5
• Molecular Formula: C₁₄H₁₆Cl₂N₈O₂
• Molecular Weight: 399.239

Synonyms:2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide

Chemical Property of 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide

Chemical Property:

Purity/Quality:

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Technology Process of 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide

There total 2 articles about 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-bis(2-bromo-2-methylpropanamido)-4,5-dichlorobenzene (136667-94-2) → 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide (136667-97-5)

Guidance literature:

With sodium azide; In ethanol; water; for 12h; Heating;

DOI:10.1021/ja00022a033

Reference yield:

4,5-Dichloro-1,2-phenylenediamine (5348-42-5) → 2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide (136667-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 73.9 percent / Et₃N / CH₂Cl₂ / 6 h

2: NaN₃ / ethanol; H₂O / 12 h / Heating

With sodium azide; triethylamine; In ethanol; dichloromethane; water;

DOI:10.1021/ja00022a033

Reference yield:

2-Azido-N-[2-(2-azido-2-methyl-propionylamino)-4,5-dichloro-phenyl]-2-methyl-propionamide (136667-97-5) → N,N'-(4,5-dichloro-1,2-phenylene)bis(2-amino-2-methylpropanamide) (136668-00-3)

Guidance literature:

With diammonium sulfide; In ethanol; water; Yield given;

DOI:10.1021/ja00022a033

upstream raw materials:

1,2-bis(2-bromo-2-methylpropanamido)-4,5-dichlorobenzene

4,5-Dichloro-1,2-phenylenediamine

Downstream raw materials:

N,N'-(4,5-dichloro-1,2-phenylene)bis(2-amino-2-methylpropanamide)

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