methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate

Base Information

• Chemical Name: methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate
• CAS No.: 651729-33-8
• Molecular Formula: C₁₉H₂₀N₂O₆S₂
• Molecular Weight: 436.51

Synonyms:methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate

Chemical Property of methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate

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Technology Process of methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate

There total 1 articles about methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Methyl [4-(2-amino-4-methoxyphenyl)aminosulfonyl-3,5-dimethylphenoxy]acetate (651729-32-7) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate (651729-33-8)

Guidance literature:

With pyridine; for 5h;

Reference yield: 80.0%

methyl [4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate (651729-33-8) + 2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride (86604-75-3) → methyl [4-[(5-methoxy-2-{[4-methoxy-3,5-dimethyl(2-pyridyl)methyl]thio}benzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate (651729-34-9)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); for 1.5h;

upstream raw materials:

Methyl [4-(2-amino-4-methoxyphenyl)aminosulfonyl-3,5-dimethylphenoxy]acetate

1,1'-Thiocarbonyldiimidazole

Downstream raw materials:

methyl [4-[(5-methoxy-2-{[4-methoxy-3,5-dimethyl(2-pyridyl)methyl]thio}benzimidazolyl)sulfonyl]-3,5-dimethylphenoxy]acetate

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