C₃₁H₅₂N₂O₇Si

Base Information

Chemical Name:C₃₁H₅₂N₂O₇Si
CAS No.:250577-85-6
Molecular Formula:C₃₁H₅₂N₂O₇Si
Molecular Weight:592.849
Hs Code.:

C<sub>31</sub>H<sub>52</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₃₁H₅₂N₂O₇Si

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Chemical Property of C₃₁H₅₂N₂O₇Si

Chemical Property:

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Technology Process of C₃₁H₅₂N₂O₇Si

There total 21 articles about C₃₁H₅₂N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 250577-84-5
C₃₁H₄₉O₇ISi

: 250577-85-6
C₃₁H₅₂N₂O₇Si

Guidance literature:: With 1-hexene; hydrazine hydrate; In ethanol; at 40 ℃; for 1h;
DOI:10.1021/ol990281j

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: 250577-85-6
C₃₁H₅₂N₂O₇Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

11.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

12.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

13.1: 126 mg / sodium iodide / acetone / 1 h / Heating

14.1: hydrazine monohydrate; 1-hexene / ethanol / 1 h / 40 °C

With 1-hexene; oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; hydrazine hydrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 250577-85-6
C₃₁H₅₂N₂O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 98 percent / imidazole / dimethylformamide / 0.5 h / 20 °C

2.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

3.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

4.1: 3.39 g / toluene / 1 h / 70 °C

5.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

5.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

7.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

8.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

9.1: 98 percent / benzene / 14 h / Heating

10.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

10.2: 78 percent / tetrahydrofuran / -78 - 20 °C

11.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

12.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

13.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

14.1: 126 mg / sodium iodide / acetone / 1 h / Heating

15.1: hydrazine monohydrate; 1-hexene / ethanol / 1 h / 40 °C

With 1H-imidazole; 1-hexene; oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; hydrazine hydrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; benzene; 3.1: Swern oxidation / 4.1: Wittig olefination / 5.2: Wittig olefination / 11.1: Wittig olefination;
DOI:10.1021/ol990281j