C₄₄H₄₄N₂P₂

Base Information

Chemical Name:C₄₄H₄₄N₂P₂
CAS No.:1334035-34-5
Molecular Formula:C₄₄H₄₄N₂P₂
Molecular Weight:662.794
Hs Code.:

C<sub>44</sub>H<sub>44</sub>N<sub>2</sub>P<sub>2</sub>

Synonyms:C₄₄H₄₄N₂P₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₄₄N₂P₂

Chemical Property:

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Technology Process of C₄₄H₄₄N₂P₂

There total 3 articles about C₄₄H₄₄N₂P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: C₄₄H₄₄N₂P₂S₂

: 1334035-34-5
C₄₄H₄₄N₂P₂

Guidance literature:: With Hexamethylphosphorous triamide; In toluene; at 100 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1002/hc.20680

Reference yield:

: 4,4'-dibutyl-2,2'-diiodoazobenzene

: 1334035-34-5
C₄₄H₄₄N₂P₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -105 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: Hexamethylphosphorous triamide / toluene / 24 h / 100 °C / Inert atmosphere; Sealed tube

With n-butyllithium; Hexamethylphosphorous triamide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/hc.20680

Reference yield:

: 1015-37-8
diphenylthiophosphinoyl chloride

: 1334035-34-5
C₄₄H₄₄N₂P₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -105 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: Hexamethylphosphorous triamide / toluene / 24 h / 100 °C / Inert atmosphere; Sealed tube

With n-butyllithium; Hexamethylphosphorous triamide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/hc.20680