Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

Base Information

Chemical Name:Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine
CAS No.:804500-76-3
Molecular Formula:C₃₁H₃₉NOSi
Molecular Weight:469.742
Hs Code.:

Synonyms:Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

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Chemical Property of Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

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Technology Process of Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

There total 2 articles about Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 100-39-0
benzyl bromide

: 804500-73-0
Allyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

: 804500-76-3
Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

Guidance literature:: With sodium carbonate; In dichloromethane; water;
DOI:10.1016/j.tet.2004.07.103

Reference yield:

: (2R,3E)-2-[(t-butyldiphenylsilyl)oxy]pent-3-ene nitrile

: 804500-76-3
Allyl-benzyl-[(E)-(R)-2-(tert-butyl-diphenyl-silanyloxy)-pent-3-enyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIBAL / diethyl ether; hexane / -78 - 0 °C

1.2: diethyl ether; hexane; methanol / -90 - 20 °C

1.3: 100 percent / sodium borohydride / diethyl ether; hexane; methanol / -20 - 20 °C

2.1: 77 percent / Na₂CO₃*10H₂O / CH₂Cl₂; H₂O

With diisobutylaluminium hydride; sodium carbonate; In diethyl ether; hexane; dichloromethane; water;
DOI:10.1016/j.tet.2004.07.103