2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Base Information

Chemical Name:2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one
CAS No.:101211-02-3
Molecular Formula:C₁₆H₂₀N₆O₅
Molecular Weight:376.372
Hs Code.:

Synonyms:2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Suppliers and Price of 2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of 2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

There total 4 articles about 2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 101211-02-3
2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / sodium hydride / toluene / 1.) 0.5 h, r.t., 2.) 70 deg C, 2 h,

2: 80 percent / lithium aluminium hydride / diethyl ether / 0 deg C, 8 deg C, r.t. overnight

3: 26 percent / conc. hydrochloric acid, 2-pentyl nitrite / acetic acid / 0 deg C, -78 deg C, 10 min, 0 deg C,

4: 1.) methanolic ammonia, 2.) triethylamine / 1.) r.t., 3 days, 2.) ethanol, reflux, 4.5 h, 0 deg C, owernight

With hydrogenchloride; lithium aluminium tetrahydride; 1-methylbutyl nitrite; ammonia; sodium hydride; triethylamine; In diethyl ether; acetic acid; toluene;

Reference yield:

: 55066-44-9
3-methyl-5-phenylpent-2-en-1-ol

: 101211-02-3
2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / conc. hydrochloric acid, 2-pentyl nitrite / acetic acid / 0 deg C, -78 deg C, 10 min, 0 deg C,

2: 1.) methanolic ammonia, 2.) triethylamine / 1.) r.t., 3 days, 2.) ethanol, reflux, 4.5 h, 0 deg C, owernight

With hydrogenchloride; 1-methylbutyl nitrite; ammonia; triethylamine; In acetic acid;

Reference yield:

: ethyl 3-methyl-5-phenylpent-2-enoate

: 101211-02-3
2-amino-6<4-hydroxy-3-hydroxyimino-2-(2-phenylethyl)-butan-2-ylamino>-5-nitropyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / lithium aluminium hydride / diethyl ether / 0 deg C, 8 deg C, r.t. overnight

2: 26 percent / conc. hydrochloric acid, 2-pentyl nitrite / acetic acid / 0 deg C, -78 deg C, 10 min, 0 deg C,

3: 1.) methanolic ammonia, 2.) triethylamine / 1.) r.t., 3 days, 2.) ethanol, reflux, 4.5 h, 0 deg C, owernight

With hydrogenchloride; lithium aluminium tetrahydride; 1-methylbutyl nitrite; ammonia; triethylamine; In diethyl ether; acetic acid;