Bis(2,4-dichlorophenyl) chlorophosphate

Base Information

Chemical Name:Bis(2,4-dichlorophenyl) chlorophosphate
CAS No.:14254-41-2
Molecular Formula:C12H6Cl5O3P
Molecular Weight:406.417
Hs Code.:2931900090
European Community (EC) Number:627-178-8
DSSTox Substance ID:DTXSID70407502
Nikkaji Number:J32.773E
Wikidata:Q72444890
Mol file:14254-41-2.mol

Synonyms:bis(2,4-dichlorophenyl) phosphorochloridate;

Suppliers and Price of Bis(2,4-dichlorophenyl) chlorophosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Bis(2,4-dichlorophenyl)Chlorophosphate
25g
$ 625.00

TRC
Bis(2,4-dichlorophenyl)Chlorophosphate
2g
$ 90.00

Oakwood
Bis(2,4-dichlorophenyl) phosphorochloridate
5g
$ 36.00

Oakwood
Bis(2,4-dichlorophenyl) phosphorochloridate
25g
$ 95.00

Oakwood
Bis(2,4-dichlorophenyl) phosphorochloridate
1g
$ 12.00

Oakwood
Bis(2,4-dichlorophenyl) phosphorochloridate
100g
$ 180.00

Matrix Scientific
Bis(2,4-dichlorophenyl) phosphorochloridate 80%
5g
$ 252.00

Matrix Scientific
Bis(2,4-dichlorophenyl) phosphorochloridate 80%
10g
$ 395.00

Matrix Scientific
Bis(2,4-dichlorophenyl) phosphorochloridate 80%
1g
$ 95.00

Biosynth Carbosynth
Bis(2,4-dichlorophenyl) chlorophosphate
2 g
$ 96.00

Total 38 raw suppliers

Chemical Property of Bis(2,4-dichlorophenyl) chlorophosphate

Chemical Property:

Vapor Pressure:9.25E-09mmHg at 25°C
Melting Point:51-56 °C(lit.)
Refractive Index:1.606
Boiling Point:475.8 °C at 760 mmHg
Flash Point:401.481 °C
PSA：45.34000
Density:1.634 g/cm³
LogP:7.10490
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), DMSO (Slightly), Ethyl Acetate (Slightly)
XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:405.846769
Heavy Atom Count:21
Complexity:367

Purity/Quality:

99%, ^*data from raw suppliers

Bis(2,4-dichlorophenyl)Chlorophosphate ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn; Xi
Hazard Codes:Xi,Xn
Statements: 36/37/38-22
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)OP(=O)(OC2=C(C=C(C=C2)Cl)Cl)Cl
Uses Bis(2,4-dichlorophenyl) chlorophosphate is a phosphate catalyst used in the direct conversion of alcohols to azides via activation. It also acts as a coupling agent in the synthesis of oligonucleotide phosphorodithioates.

Technology Process of Bis(2,4-dichlorophenyl) chlorophosphate

There total 4 articles about Bis(2,4-dichlorophenyl) chlorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.1%

: 14254-41-2
bis(2,4-dichlorodiphenyl) phosphorochloridate

Guidance literature:

Reference yield: 45.0%

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 19430-75-2
2,4-dichlorophenylphosphorodichloridate

: 14254-41-2
bis(2,4-dichlorodiphenyl) phosphorochloridate

Guidance literature:: With magnesium; trichlorophosphate; for 6h; Heating;
DOI:10.1021/ja00175a030

Reference yield:

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 14254-41-2
bis(2,4-dichlorodiphenyl) phosphorochloridate

Guidance literature:: Multi-step reaction with 2 steps

1: 14.20 g / phosphoryl chloride, magnesium / 6 h / Heating

2: 7.53 g / magnesium / 5 h / Heating

With magnesium; trichlorophosphate;
DOI:10.1021/ja00175a030