2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

Base Information

• Chemical Name: 2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester
• CAS No.: 868632-01-3
• Molecular Formula: C₁₉H₂₂N₂O₄S
• Molecular Weight: 374.461

Synonyms:2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

Chemical Property of 2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

Chemical Property:

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Technology Process of 2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

There total 1 articles about 2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1-benzyl-4-oxo-piperidine-3-carboxylic acid methyl ester (57611-47-9) + ethyl 2-cyanoacetate (105-56-6) → 2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester (868632-01-3)

Guidance literature:

1-benzyl-4-oxo-piperidine-3-carboxylic acid methyl ester; ethyl 2-cyanoacetate; With sulfur; In ethanol; at 50 ℃;

With diethylamine; In ethanol; at 60 ℃;

DOI:10.1002/ardp.200700205

Reference yield: 82.0%

2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester (868632-01-3) + Benzoyl isothiocyanate (532-55-8) → 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester (1050207-41-4)

Guidance literature:

In acetone; for 2h; Reflux;

DOI:10.1002/ardp.200700205

upstream raw materials:

1-benzyl-4-oxo-piperidine-3-carboxylic acid methyl ester

ethyl 2-cyanoacetate

Downstream raw materials:

2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

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