2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

Base Information

Chemical Name:2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester
CAS No.:1050207-41-4
Molecular Formula:C₂₇H₂₇N₃O₅S₂
Molecular Weight:537.66
Hs Code.:

Synonyms:2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

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Chemical Property of 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

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Technology Process of 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

There total 1 articles about 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 868632-01-3
2-amino-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

: 532-55-8
Benzoyl isothiocyanate

: 1050207-41-4
2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

Guidance literature:: In acetone; for 2h; Reflux;
DOI:10.1002/ardp.200700205

Reference yield: 66.0%

: 1050207-41-4
2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

: 74-88-4
methyl iodide

: 1050207-62-9
2-(methylthio)-7-(phenylmethyl)-4-oxo-1,4,5,6,7,8-hexahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidine-5-carboxylic acid methyl ester

Guidance literature:: 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester; With potassium hydroxide; In ethanol; for 3h; Reflux;

methyl iodide; In water; at 20 ℃; for 1.5h;
DOI:10.1002/ardp.200700205

Reference yield: 26.0%

: 1050207-41-4
2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester

: 1050207-54-9
7-(phenylmethyl)-4-oxo-2-thioxo-1,2,3,4,5,6,7,8-octahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidine-5-carboxylic acid methyl ester

Guidance literature:: 2-[[(benzoylamino)thioxomethyl]amino]-6-(phenylmethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,4-dicarboxylic acid 3-ethyl 4-methyl diester; With potassium hydroxide; In ethanol; for 3h; Reflux;

With hydrogenchloride; In water; at 20 ℃; for 0.5h;
DOI:10.1002/ardp.200700205