Technology Process of C17H17BrO4
There total 5 articles about C17H17BrO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate; sodium iodide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; magnesium chloride / acetonitrile / 0.5 h / Inert atmosphere; Reflux
2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
With
caesium carbonate; triethylamine; sodium iodide; magnesium chloride;
In
N,N-dimethyl-formamide; acetonitrile;
1: Casiraghi/Hoflokken ortho-formylation;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bromine / chloroform / Inert atmosphere
2: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / Inert atmosphere
3: triethylsilane; trifluoroacetic acid / dichloromethane / 5.5 h / 0 °C / Inert atmosphere
4: triethylamine; magnesium chloride / acetonitrile / 0.5 h / Inert atmosphere; Reflux
5: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
With
triethylsilane; bromine; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; caesium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; magnesium chloride;
In
dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;
4: Casiraghi/Hoflokken ortho-formylation;
DOI:10.1016/j.tet.2011.04.094
