(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Base Information

Chemical Name:(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine
CAS No.:336195-57-4
Molecular Formula:C₂₈H₃₈N₂O₄
Molecular Weight:466.621
Hs Code.:

Synonyms:(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Suppliers and Price of (R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Chemical Property:

Purity/Quality:

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Technology Process of (R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

There total 4 articles about (R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32044-22-7,39961-95-0
(1R,2R)-1,2-diaminocyclohexane tartrate

: 192803-37-5
3-tert-butyl-2,5-dihydroxybenzaldehyde

: 336195-57-4
(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; for 2h; Reflux;
DOI:10.1016/j.tet.2014.03.043

Reference yield:

: 1948-33-0
tert-butylhydroquinone

: 336195-57-4
(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole; dmap / dichloromethane / 18 h / 0 - 4 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine; tin(IV) chloride / toluene / 1 h / 0 °C / Inert atmosphere

2.2: 24 h / 90 °C / Inert atmosphere

3.1: potassium hydroxide / ethanol; water / 5 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / water; tetrahydrofuran / 2 h / Reflux

With 1H-imidazole; 2,6-dimethylpyridine; dmap; tin(IV) chloride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2014.03.043

Reference yield:

: 246509-53-5
2-hydroxy-5-pivaloyloxy-3-tert-butylbenzaldehyde

: 336195-57-4
(R,R)-N,N′-bis(3-tert-butyl-5-hydroxysalicylidene)-1,2-cyclohexanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water / 5 h / 20 °C / Inert atmosphere

2: potassium carbonate / water; tetrahydrofuran / 2 h / Reflux

With potassium carbonate; potassium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.tet.2014.03.043