(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Base Information

Chemical Name:(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester
CAS No.:685508-76-3
Molecular Formula:C₂₃H₂₆N₂O₉S
Molecular Weight:506.533
Hs Code.:

Synonyms:(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Suppliers and Price of (S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

There total 3 articles about (S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3883-94-1
2-amino-4'-methoxyacetophenone hydrochloride

: (S)-2-(4-Chlorocarbonyl-benzenesulfonylamino)-pentanedioic acid dimethyl ester

: 685508-76-3
(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Guidance literature:: With sodium hydrogencarbonate; In toluene; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2003.12.076

Reference yield:

: 129972-93-6
C₁₁H₁₁NO₄

: 685508-76-3
(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / HCl / methanol / 48 h / 20 °C

2: 90 percent / aq. NaHCO₃ / toluene / 1 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; In methanol; toluene;
DOI:10.1016/j.bmcl.2003.12.076

Reference yield:

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 685508-76-3
(S)-2-{4-[2-(4-Methoxy-phenyl)-2-oxo-ethylcarbamoyl]-benzenesulfonylamino}-pentanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / acetonitrile / 3 h / 20 °C

2: 92 percent / HCl / methanol / 48 h / 20 °C

3: 90 percent / aq. NaHCO₃ / toluene / 1 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; In methanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2003.12.076