methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

Base Information

Chemical Name:methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate
CAS No.:360556-73-6
Molecular Formula:C₁₅H₂₄O₇S₂
Molecular Weight:380.483
Hs Code.:

Synonyms:methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

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Chemical Property of methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

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Technology Process of methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

There total 5 articles about methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124-63-0
methanesulfonyl chloride

: 360556-72-5
3-[3-(3-hydroxypropyl)-2-methoxyphenyl]propanol

: 360556-73-6
methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1002/1099-0682(200107)2001:7<1763::AID-EJIC1763>3.0.CO;2-F

Reference yield:

: 144587-96-2
3-[3-(2-carboxyethyl)-2-methoxyphenyl]propionic acid

: 360556-73-6
methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / p-toluenesulfonic acid / 12 h / Heating

2: 91 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

3: 95 percent / triethylamine / CH₂Cl₂ / 2 h / 0 °C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1002/1099-0682(200107)2001:7<1763::AID-EJIC1763>3.0.CO;2-F

Reference yield:

: 360556-71-4
ethyl 3-[3-(2-ethoxycarbonylethyl)-2-methoxyphenyl]propionate

: 360556-73-6
methyl 3-[2-methoxy-3-(3-methylsulfonyloxypropyl)phenyl]propylsulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

2: 95 percent / triethylamine / CH₂Cl₂ / 2 h / 0 °C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1002/1099-0682(200107)2001:7<1763::AID-EJIC1763>3.0.CO;2-F