p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

Base Information

Chemical Name:p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol
CAS No.:137601-89-9
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:

Synonyms:p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

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Chemical Property of p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

Chemical Property:

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Technology Process of p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

There total 4 articles about p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 64-17-5
ethanol

: 42427-46-3
p-(1-Methylcyclopropyl)acetophenone

: 1-(1-ethoxyethyl)-4-(1-methylcyclopropyl)benzene

: 137601-89-9
p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

Guidance literature:: ethanol; p-(1-Methylcyclopropyl)acetophenone; With sodium tetrahydroborate; at 20 ℃;

With hydrogenchloride; In water; at 60 ℃; for 10h;
DOI:10.1134/S1070428016040047

Reference yield: 79.0%

: 42427-46-3
p-(1-Methylcyclopropyl)acetophenone

: 137601-89-9
p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

Guidance literature:: With sodium tetrahydroborate;
DOI:10.1134/S107042801509002X

Reference yield:

: 2214-14-4
(1-methylcyclopropyl)benzene

: 137601-89-9
p-(1-Methylcyclopropyl)-α-methylbenzyl Alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / aluminium(III) chloride / CHCl₃ / 7 °C

2: NaBH₄ / propan-2-ol / Ambient temperature; or with LiAlH₄ in ether at 3 degC

With sodium tetrahydroborate; aluminium trichloride; In chloroform; isopropyl alcohol;
DOI:10.1246/bcsj.64.2954