Technology Process of C42H46O10Si
There total 15 articles about C42H46O10Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at -20 - 20 ℃;
for 3h;
Inert atmosphere;
Industry scale;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Industry scale
2: trifluoroacetic acid / 4 h / 20 °C / Industry scale
3: 1H-imidazole / dichloromethane / 3 h / 20 °C / Inert atmosphere; Industry scale
4: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere; Industry scale
With
pyridine; 1H-imidazole; dmap; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 10 - 20 °C / Inert atmosphere
2: trifluoroacetic acid / 5 °C
3: 1H-imidazole / dichloromethane / 3 h / -20 - 20 °C
4: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
dmap;
In
tetrahydrofuran; dichloromethane;