CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4

Base Information

• Chemical Name: CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4
• CAS No.: 227005-28-9
• Molecular Formula: C₂₄H₂₀B*C₄₉H₄₉IrP₃S
• Molecular Weight: 1274.37
• Mol file: 227005-28-9.mol

Synonyms:CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4

Chemical Property of CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4

There total 1 articles about CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)⁽¹⁺⁾*B(C₆H₅)4^(1-)=CH₃C[CH₂P(C₆H₅)2]3IrH₂(C₈SH₈)B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,3-dihydrobenzo(b)thiophene (4565-32-6) + [(1,1,1-tris(diphenylphosphinomethyl)ethane)Ir(H)2(THF)]BPh4 (142928-68-5) → CH3C[CH2P(C6H5)2]3IrH2(C8SH8)(1+)*B(C6H5)4(1-)=CH3C[CH2P(C6H5)2]3IrH2(C8SH8)B(C6H5)4 (227005-28-9)

Guidance literature:

In tetrahydrofuran; react. at room temp.;

DOI:10.1039/a900959k

Reference yield:

CH3C[CH2P(C6H5)2]3IrH2(C8SH8)(1+)*B(C6H5)4(1-)=CH3C[CH2P(C6H5)2]3IrH2(C8SH8)B(C6H5)4 (227005-28-9) → CH3C[CH2P(C6H5)2]3IrH2(SC6H4CHCH2) (227005-29-0)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran-d8; byproducts: (CH3)3COH; react. at 20°C;

DOI:10.1039/a900959k

upstream raw materials:

2,3-dihydrobenzo(b)thiophene

[(1,1,1-tris(diphenylphosphinomethyl)ethane)Ir(H)2(THF)]BPh₄

Downstream raw materials:

CH₃C[CH₂P(C₆H₅)2]3IrH₂(SC₆H₄CHCH₂)