5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid

Base Information

• Chemical Name: 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid
• CAS No.: 54114-81-7
• Molecular Formula: C₃₂H₂₄Cl₂N₁₀O₆S₂
• Molecular Weight: 779.644
• Mol file: 54114-81-7.mol

Synonyms:5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid

Chemical Property of 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid

There total 3 articles about 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5'-bis-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid (16013-46-0) + aniline (62-53-3) → 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid (54114-81-7)

Guidance literature:

With sodium hydroxide; In water; at 45 ℃; for 4h; pH=6 - 7; Inert atmosphere;

Reference yield:

4,4'-diaminostilbene-2,2'-disulfonic acid (81-11-8) → 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid (54114-81-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water / 2 h / 0 °C / pH 4 - 5 / Inert atmosphere

2: sodium hydroxide / water / 4 h / 45 °C / pH 6 - 7 / Inert atmosphere

With sodium hydroxide; In water;

Reference yield:

→ 5,5'-bis-(4-anilino-6-chloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid (54114-81-7)

Guidance literature:

entspr.2,4-Dichloro-1,3,5-triazin(2)/4,4'-Diamino-2,2'-stilbendisulfonsaeure;

upstream raw materials:

4,4'-diaminostilbene-2,2'-disulfonic acid

5,5'-bis-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-2,2'-ethene-1,2-diyl-bis-benzenesulfonic acid

aniline