N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

Base Information

Chemical Name:N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate
CAS No.:252668-51-2
Molecular Formula:C₁₇H₁₆ClNO₄S
Molecular Weight:365.837
Hs Code.:

Synonyms:N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

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Chemical Property of N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

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Technology Process of N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

There total 3 articles about N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 106-47-8
4-chloro-aniline

: 252668-49-8
(E)-2-(methylsulfonyl)-3-phenyl-2-propenyl chloroformate

: 252668-51-2
N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/jo990541a

Reference yield:

: 197244-90-9
(E)-2-(methylsulfonyl)-3-phenyl-2-propenyl alcohol

: 252668-51-2
N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 86.4 percent / tetrahydrofuran / 20 °C

2: 90 percent / DIEA / CH₂Cl₂ / 1.5 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Substitution / 2: Substitution;
DOI:10.1021/jo990541a

Reference yield:

: (E)-3-bromo-2-(methylsulfonyl)-1-phenyl-1-propene

: 252668-51-2
N-p-chlorophenyl (E)-2-(methylsulfonyl)-3-phenyl-2-propenyl carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 80.2 percent / sodium formate; H₂O / methanol / 6 h / Heating

2: 86.4 percent / tetrahydrofuran / 20 °C

3: 90 percent / DIEA / CH₂Cl₂ / 1.5 h / 20 °C

With water; sodium formate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1021/jo990541a