AMD-5cis

Base Information

Chemical Name:AMD-5cis
CAS No.:1357001-71-8
Molecular Formula:C₃₃H₃₄FN₃O
Molecular Weight:507.651
Hs Code.:

Synonyms:AMD-5cis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of AMD-5cis

Chemical Property:

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Technology Process of AMD-5cis

There total 4 articles about AMD-5cis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1357001-59-2
AMN-2cis

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 1357001-71-8
AMD-5cis

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 20 ℃;

Reference yield:

: 863514-54-9
4-(dimethylamino)-4-(3-fluorophenyl)cyclohexan-1-one

: 61-54-1
tryptamine

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 1357001-81-0
cis-(E)-4-(3-fluorophenyl)-2’,3’,4’,9’-tetrahydro-N,N-dimethyl-2’-(1-oxo-3-phenyl-2-propenyl)spiro[cyclohexane-1,1’[1H]-pyrido[3,4-b]indol]-4-amine

: 1357001-71-8
AMD-5cis

Guidance literature:: 4-(dimethylamino)-4-(3-fluorophenyl)cyclohexan-1-one; tryptamine; In methanol; for 24h; Inert atmosphere;

With trifluoroacetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 2h;

Cinnamoyl chloride;

Reference yield:

: 1002916-54-2
[8-(3-Fluoro-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yl]-dimethyl-amine hydrochloride

: 1357001-71-8
AMD-5cis

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / 96 h / 20 °C

1.2: cooling with ice

2.1: methanol / 24 h / Inert atmosphere

2.2: 2 h / 20 °C

2.3: pH 11

3.1: N-ethyl-N,N-diisopropylamine / 20 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In methanol;