phytanyl 1-benzyl heptaethylene glycol succinate

Base Information

Chemical Name:phytanyl 1-benzyl heptaethylene glycol succinate
CAS No.:423763-17-1
Molecular Formula:C₄₅H₈₀O₁₁
Molecular Weight:797.124
Hs Code.:

Synonyms:phytanyl 1-benzyl heptaethylene glycol succinate

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Chemical Property of phytanyl 1-benzyl heptaethylene glycol succinate

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Technology Process of phytanyl 1-benzyl heptaethylene glycol succinate

There total 6 articles about phytanyl 1-benzyl heptaethylene glycol succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 423763-19-3
monobenzyl heptaethylene glycol

: 199484-61-2
phytanyl hemisuccinate

: 423763-17-1
phytanyl 1-benzyl heptaethylene glycol succinate

Guidance literature:: With dmap; Morpho-CDI; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1071/CH01111

Reference yield:

: 112-60-7
Tetraethylene glycol

: 423763-17-1
phytanyl 1-benzyl heptaethylene glycol succinate

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / 40 percent aq. NaOH / 24 h / 100 °C

2: 71 percent / NaH / tetrahydrofuran / 24 h / 20 °C

3: 100 percent / 10 M HCl / CH₂Cl₂; methanol / 6 h / 20 °C

4: 36 percent / DMAP; morpho-CDI / CH₂Cl₂ / 16 h / 20 °C

With hydrogenchloride; dmap; sodium hydroxide; Morpho-CDI; sodium hydride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1071/CH01111

Reference yield:

: 189302-44-1
(3RS,7R,11R)-3,7,11,15-tetramethylhexadecan-1-ol

: 423763-17-1
phytanyl 1-benzyl heptaethylene glycol succinate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 3 h / Heating

2: 36 percent / DMAP; morpho-CDI / CH₂Cl₂ / 16 h / 20 °C

With dmap; Morpho-CDI; triethylamine; In dichloromethane;
DOI:10.1071/CH01111