4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

Base Information

Chemical Name:4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide
CAS No.:1055927-20-2
Molecular Formula:C₂₀H₂₀ClN₇O
Molecular Weight:409.878
Hs Code.:

Synonyms:4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

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Chemical Property of 4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

Chemical Property:

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Technology Process of 4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

There total 2 articles about 4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 876-08-4
p-(chloromethyl)benzoyl chloride

: 1055927-17-7
6-(1-cyclohexylhydrazino)-1H-purine-2-carbonitrile

: 1055927-20-2
4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 1055927-13-3
1,1-dimethylethyl 2-[2-chloro-9-(tetrahydro-2H-pyran-2-yl)-9H-purin-6-yl]-2-cyclohexylhydrazinecarboxylate

: 1055927-20-2
4-(chloromethyl)-N'-(2-cyano-1H-purin-6-yl)-N'-cyclohexyl benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-bis-(diphenylphosphino)ferrocene; zinc / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / ISOPROPYLAMIDE / 150 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; N-ethyl-N,N-diisopropylamine; zinc; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; ISOPROPYLAMIDE;