chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride

Base Information

• Chemical Name: chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride
• CAS No.: 848029-39-0
• Molecular Formula: C₁₉H₁₀Cl₂O₂S₃
• Molecular Weight: 437.391
• Mol file: 848029-39-0.mol

Synonyms:chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride

Chemical Property of chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride

There total 1 articles about chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4,5-dichloro-1,2-dithiole-3-thione (57248-64-3) + 1,4-diphenyl-but-2-yne-1,4-dione (1087-09-8) → chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride (848029-39-0)

Guidance literature:

In xylene; at 20 ℃; for 10h;

DOI:10.1021/ol0476669

Reference yield:

chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride (848029-39-0) + dimethyl acetylenedicarboxylate (762-42-5) → 2,3-dibenzoyl-4-thioxo-4H-thieno[3,2-c]thiopyran-6,7-dicarboxylic acid dimethyl ester + 2,3-dibenzoyl-7-thioxo-7H-thieno[2,3-c]thiopyran-4,5-dicarboxylic acid dimethyl ester

Guidance literature:

In xylene; Heating;

DOI:10.1021/ol0476669

Reference yield:

chloro-(4,5-dibenzoyl-[1,3]dithiol-2-ylidene)-thioacetyl chloride (848029-39-0) + 1,4-diphenyl-but-2-yne-1,4-dione (1087-09-8) → phenyl-(2,6,7-tribenzoyl-4-thioxo-4H-thieno[3,2-c]thiopyran-3-yl)-methanone + phenyl-(2,4,5-tribenzoyl-7-thioxo-7H-thieno[2,3-c]thiopyran-3-yl)-methanone

Guidance literature:

In xylene; Heating;

DOI:10.1021/ol0476669

upstream raw materials:

4,5-dichloro-1,2-dithiole-3-thione

1,4-diphenyl-but-2-yne-1,4-dione