N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

Base Information

Chemical Name:N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine
CAS No.:135227-37-1
Molecular Formula:C₂₅H₃₁F₃N₂O₅
Molecular Weight:496.527
Hs Code.:

Synonyms:N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

Suppliers and Price of N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

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Technology Process of N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

There total 2 articles about N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79722-21-7
tert-butyl N-(benzyloxy)carbamate

: 135227-37-1
N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, room temperature, 15 min, 2.) 0 deg C to room temperature, several h

2: 1.) NaH / 1.) DMF, room temperature, 1 h, 2.) 70-80 deg C, 18 h

With sodium hydride;
DOI:10.1021/jo00019a017

Reference yield:

: 354-38-1
2,2,2-trifluoroacetamide

: 135256-18-7
O-Benzyl-N-(tert-butoxycarbonyl)-N-<4-(tosyloxy)-3(S)-(benzyloxy)butyl>hydroxylamine

: 135227-37-1
N-(Trifluoroacetyl)-N'-(tert-butoxycarbonyl)-N',2(S)-bis(benzyloxy)-1,4-butanediamine

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, room temperature, 1 h, 2.) 70-80 deg C, 18 h;
DOI:10.1021/jo00019a017