⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

Base Information

Chemical Name:⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate
CAS No.:1384626-56-5
Molecular Formula:C₁₇H₂₄N₂O₅
Molecular Weight:340.344
Hs Code.:

<sup>(13)</sup>C<sub>4</sub>-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

Synonyms:⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

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Chemical Property of ⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

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Technology Process of ⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

There total 5 articles about ⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 1384626-56-5
⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / methanol / 3 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 0 - 20 °C

3.1: triethylamine / 1,4-dioxane; water / 2 h / 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

6.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

6.2: 2 h / 20 °C

With sodium tetrahydroborate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.05.084

Reference yield:

: 1384626-47-4
1,2-⁽¹³⁾C₂-methyl 2-(benzyl(tert-butoxycarbonyl)amino)acetate

: 1384626-56-5
⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

2.2: 2 h / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.tetlet.2012.05.084

Reference yield:

: 1384626-43-0
1,2-⁽¹³⁾C₂-2-(benzylamino)acetic acid

: 1384626-56-5
⁽¹³⁾C₄-methyl 2-(N-benzyl-2-(tert-butoxycarbonylamino)acetamido)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / 1,4-dioxane; water / 2 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

4.2: 2 h / 20 °C

With caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.05.084