S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

Base Information

Chemical Name:S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate
CAS No.:1430198-72-3
Molecular Formula:C₂₈H₂₀N₂O₂S₂
Molecular Weight:480.611
Hs Code.:

Synonyms:S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

Suppliers and Price of S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

There total 2 articles about S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1430198-69-8
7-[4-(tert-butylthio)phenyl]-2-(4-(tert-butylthio)phenyl)-1,8a-dihydroazulene-1,1-dicarbonitrile

: 75-36-5
acetyl chloride

: 1430198-72-3
S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

Guidance literature:: With bismuth(lll) trifluoromethanesulfonate; In toluene; acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1002/ejoc.201500420

Reference yield:

: 1430198-69-8
7-[4-(tert-butylthio)phenyl]-2-(4-(tert-butylthio)phenyl)-1,8a-dihydroazulene-1,1-dicarbonitrile

: 75-36-5
acetyl chloride

: 1430198-72-3
S,S'-[(3,3-dicyano-3,3a-dihydroazulene-2,5-diyl)bis(4,1-phenylene)] diethanethioate

: 1430198-84-7
C₂₈H₂₀N₂O₂S₂

Guidance literature:: With boron tribromide; In dichloromethane; toluene; for 6h; Overall yield = 75%; Overall yield = 96 mg;
DOI:10.1021/jo400362u