Technology Process of C53H94NO7(1+)*Cl(1-)
There total 8 articles about C53H94NO7(1+)*Cl(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
1,4-dioxane;
at 0 - 55 ℃;
for 3h;
Inert atmosphere;
Basic conditions;
DOI:10.1021/ja106707z
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
2: tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere
3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / Inert atmosphere
4: 6 h / 80 °C / Inert atmosphere
5: 1,4-dioxane / 3 h / 0 - 55 °C / Inert atmosphere; Basic conditions
With
thionyl chloride; dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/ja106707z
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / tert-butyl methyl ether / 2.17 h / 0 - 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: thionyl chloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
3.1: tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere
4.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / Inert atmosphere
5.1: 6 h / 80 °C / Inert atmosphere
6.1: 1,4-dioxane / 3 h / 0 - 55 °C / Inert atmosphere; Basic conditions
With
lithium aluminium tetrahydride; thionyl chloride; dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; tert-butyl methyl ether; water;
DOI:10.1021/ja106707z
