C₅₀H₆₉ClN₁₀O₁₁

Base Information

Chemical Name:C₅₀H₆₉ClN₁₀O₁₁
CAS No.:1613707-48-4
Molecular Formula:C₅₀H₆₉ClN₁₀O₁₁
Molecular Weight:1021.61
Hs Code.:

C<sub>50</sub>H<sub>69</sub>ClN<sub>10</sub>O<sub>11</sub>

Synonyms:C₅₀H₆₉ClN₁₀O₁₁

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Chemical Property of C₅₀H₆₉ClN₁₀O₁₁

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Technology Process of C₅₀H₆₉ClN₁₀O₁₁

There total 18 articles about C₅₀H₆₉ClN₁₀O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 76942-92-2
methyl 3,5-diamino-6-chloropyrazine-2-carbonylcarbamimidothioate hydroiodic acid salt

: C₄₄H₆₄N₄O₁₀*2C₂H₄O₂

: 1613707-48-4
C₅₀H₆₉ClN₁₀O₁₁

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 70 ℃; for 2h; Sealed tube;

Reference yield:

: (Z)-methyl 2-(tert-butyloxycarbonyl)amino-3-(1-(tert-butyldimethylsilyloxy)naphthalen-4-yl)acrylate

: 1613707-48-4
C₅₀H₆₉ClN₁₀O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

3: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

4: pyridine / 2 h / 0 - 20 °C

5: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

6: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

7: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

9: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 70 °C / Sealed tube

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1613707-21-3
methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldimethylsilyloxy)naphthalen-1-yl)propanoate

: 1613707-48-4
C₅₀H₆₉ClN₁₀O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

2: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

3: pyridine / 2 h / 0 - 20 °C

4: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

5: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

7: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

8: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 70 °C / Sealed tube

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;