(cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

Base Information

Chemical Name:(cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate
CAS No.:99225-34-0
Molecular Formula:C₃₆H₃₆NOPRh*ClO₄
Molecular Weight:732.018
Hs Code.:

Synonyms:(cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

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Chemical Property of (cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

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Technology Process of (cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

There total 2 articles about (cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 99243-78-4
(cyclooctadiene)bis(4-methylquinoline N-oxide)rhodium(I) perchlorate

: 99225-34-0
(cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

Guidance literature:: With P(C₆H₅)3; In dichloromethane; Rh-complex in CH2Cl2 was treated with PPh3, mixt. was stirred for 0.5 hin air at room temp.; filtered, filtrate was concd., Et2O was added, stirred, cooled to -5°C, ppt. was dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)87968-2

Reference yield:

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 99225-34-0
(cyclooctadiene)(4-methylquinoline N-oxide)(triphenylphosphine)rhodium(I) perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: acetone

2: P(C₆H₅)3 / dichloromethane

With P(C₆H₅)3; In dichloromethane; acetone;
DOI:10.1016/S0020-1693(00)87968-2