DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

Base Information

Chemical Name:DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol
CAS No.:125258-18-6
Molecular Formula:C₅₄H₅₀O₆
Molecular Weight:794.987
Hs Code.:

Synonyms:DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

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Chemical Property of DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

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Technology Process of DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

There total 4 articles about DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 532-32-1
sodium benzoate

: 125258-14-2
Methanesulfonic acid (1R,2S,3R,4R,6S)-2,3,4-tris-benzyloxy-6-trityloxymethyl-cyclohexyl ester

: 125258-18-6
DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 12h;
DOI:10.1016/0008-6215(89)85057-8

Reference yield:

: 117902-49-5
(1RS,6RS,8RS,9SR,10SR)-8,9,10-trobenzyloxy-3,3-dimethyl-2,4-dioxabicyclo<4.4.0>decane

: 125258-18-6
DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / 50percent AcOH, / ethanol; H₂O / 3.5 h / Ambient temperature

2: 85 percent / pyridine / 18 h / 60 °C

3: 75 percent / pyridine / 48 h / 45 °C

4: 95 percent / dimethylformamide / 12 h / 120 °C

With acetic acid; In pyridine; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85057-8

Reference yield:

: 125258-11-9,125354-35-0
DL-(1,2/3,4,5)-1,2,3-tri-O-benzyl-5-hydroxymethyl-1,2,3,4-cyclohexanetetrol

: 125258-18-6
DL-(1,2,4/3,5)-4-O-benzoyl-1,2,3-tri-O-benzyl-5-trityloxymethyl-1,2,3,4-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine / 18 h / 60 °C

2: 75 percent / pyridine / 48 h / 45 °C

3: 95 percent / dimethylformamide / 12 h / 120 °C

In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85057-8