C₂₂H₂₂IN

Base Information

Chemical Name:C₂₂H₂₂IN
CAS No.:1573172-23-2
Molecular Formula:C₂₂H₂₂IN
Molecular Weight:427.328
Hs Code.:

Synonyms:C₂₂H₂₂IN

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Chemical Property of C₂₂H₂₂IN

Chemical Property:

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Technology Process of C₂₂H₂₂IN

There total 6 articles about C₂₂H₂₂IN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65658-16-4
2-amino-6-methylbenzyl alcohol

: 1573172-23-2
C₂₂H₂₂IN

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / acetone / 0.5 h / 0 °C

1.2: 1.5 h

2.1: phosphorus tribromide / tetrachloromethane / 2 h / 0 °C

3.1: N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux

With hydrogenchloride; phosphorus tribromide; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; acetone; toluene;
DOI:10.1021/ja412706d

Reference yield:

: 13506-76-8
2-methyl-6-nitrobenzoic acid

: 1573172-23-2
C₂₂H₂₂IN

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetone / 14 h / Reflux

2.1: hydrogen; palladium 10% on activated carbon / methanol / 24 h / 20 °C / 760.05 Torr

3.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

4.1: hydrogenchloride / acetone / 0.5 h / 0 °C

4.2: 1.5 h

5.1: phosphorus tribromide / tetrachloromethane / 2 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux

With hydrogenchloride; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; phosphorus tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; tetrachloromethane; diethyl ether; acetone; toluene;
DOI:10.1021/ja412706d

Reference yield:

: 18595-13-6
2-amino-6-methylbenzoic acid methyl ester

: 1573172-23-2
C₂₂H₂₂IN

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C

2.1: hydrogenchloride / acetone / 0.5 h / 0 °C

2.2: 1.5 h

3.1: phosphorus tribromide / tetrachloromethane / 2 h / 0 °C

4.1: N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus tribromide; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; diethyl ether; acetone; toluene;
DOI:10.1021/ja412706d