Technology Process of C19H24BF2N3O2
There total 8 articles about C19H24BF2N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: Dess-Martin periodane / dichloromethane / 7 h / 0 - 20 °C
2: diethylamino-sulfur trifluoride / dichloromethane / 21 h / -78 - 20 °C
3: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C
4: trifluoroacetic acid / dichloromethane
5: ammonium acetate / toluene / 5 h / 110 °C
6: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane; water / 2 h / 90 °C / Inert atmosphere
7: hydrogenchloride / ethyl acetate / 8 h / 20 °C
With
hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; diethylamino-sulfur trifluoride; ammonium acetate; water; potassium acetate; Dess-Martin periodane; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / dichloromethane
2: ammonium acetate / toluene / 5 h / 110 °C
3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane; water / 2 h / 90 °C / Inert atmosphere
4: hydrogenchloride / ethyl acetate / 8 h / 20 °C
With
hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ammonium acetate; potassium acetate; trifluoroacetic acid;
In
1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; toluene;