4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Base Information

Chemical Name:4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol
CAS No.:191488-00-3
Molecular Formula:C₆₅H₈₄O₈S₃
Molecular Weight:1089.58
Hs Code.:

4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Synonyms:4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Suppliers and Price of 4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

There total 22 articles about 4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 191487-99-7
C₇₃H₉₂O₁₆S₃

: 191488-00-3
4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Guidance literature:: With caesium carbonate; thiophenol; In N,N-dimethyl-formamide; at 85 ℃;

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 191488-00-3
4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Guidance literature:: Multi-step reaction with 10 steps

1: 80 percent / dimethylformamide / 20 °C

2: 89 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 0 °C

3: 86 percent / Al(Oi-Pr)3 / toluene / 110 °C

4: 71 percent / t-BuOK / dimethylformamide / -20 °C

5: 92 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

6: 90 percent / diethylaniline, pyridine / benzene / 25 °C

7: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

8: 96 percent / diethylaniline, pyridine / benzene / 25 °C

9: 80 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

10: 82 percent / C₆H₅SH, Cs₂CO₃ / dimethylformamide / 85 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; aluminum isopropoxide; caesium carbonate; thiophenol; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; benzene;

Reference yield:

: 106-24-1
Geraniol

: 191488-00-3
4-Methoxy-2-((2E,6E,10E,14E,18E,22E,26E)-5,13,21-tris-benzenesulfonyl-3,7,11,15,19,23,27,31-octamethyl-dotriaconta-2,6,10,14,18,22,26,30-octaenyl)-phenol

Guidance literature:: Multi-step reaction with 11 steps

1: 90 percent / PBr₃ / diethyl ether / -20 °C

2: 80 percent / dimethylformamide / 20 °C

3: 89 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 0 °C

4: 86 percent / Al(Oi-Pr)3 / toluene / 110 °C

5: 71 percent / t-BuOK / dimethylformamide / -20 °C

6: 92 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

7: 90 percent / diethylaniline, pyridine / benzene / 25 °C

8: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

9: 96 percent / diethylaniline, pyridine / benzene / 25 °C

10: 80 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

11: 82 percent / C₆H₅SH, Cs₂CO₃ / dimethylformamide / 85 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; phosphorus tribromide; aluminum isopropoxide; caesium carbonate; thiophenol; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; benzene;