C₁₂H₁₆Cl₂O

Base Information

Chemical Name:C₁₂H₁₆Cl₂O
CAS No.:1351663-14-3
Molecular Formula:C₁₂H₁₆Cl₂O
Molecular Weight:247.164
Hs Code.:

C<sub>12</sub>H<sub>16</sub>Cl<sub>2</sub>O

Synonyms:C₁₂H₁₆Cl₂O

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Chemical Property of C₁₂H₁₆Cl₂O

Chemical Property:

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Technology Process of C₁₂H₁₆Cl₂O

There total 4 articles about C₁₂H₁₆Cl₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 56-23-5
tetrachloromethane

: 1351663-03-0
C₁₁H₁₆O₂

: 1351663-14-3
C₁₂H₁₆Cl₂O

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; for 6h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.09.103

Reference yield:

: 1351662-99-1
C₁₂H₁₉NO₄

: 1351663-14-3
C₁₂H₁₆Cl₂O

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / Inert atmosphere

2: triphenylphosphine / tetrahydrofuran / 6 h / Inert atmosphere; Reflux

With water; acetic acid; triphenylphosphine; In tetrahydrofuran; 2: Wittig type condensation;
DOI:10.1016/j.tet.2011.09.103

Reference yield:

: 589-92-4
1-methylcyclohexan-4-one

: 1351663-14-3
C₁₂H₁₆Cl₂O

Guidance literature:: Multi-step reaction with 4 steps

1: ethylenediamine / 7 h / Inert atmosphere; Reflux

2: potassium fluoride / methanol / 4 h / Inert atmosphere; Reflux

3: water; acetic acid / Inert atmosphere

4: triphenylphosphine / tetrahydrofuran / 6 h / Inert atmosphere; Reflux

With potassium fluoride; water; acetic acid; ethylenediamine; triphenylphosphine; In tetrahydrofuran; methanol; 2: Michael addition / 4: Wittig type condensation;
DOI:10.1016/j.tet.2011.09.103