Technology Process of C17H22N2O4
There total 5 articles about C17H22N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: isobutyl chloroformate; N-methylmorpholine / tetrahydrofuran
1.2: diethyl ether
2.1: TEA / silver benzoate
3.1: H2 / Pd/C / methanol
3.2: tetrahydrofuran
4.1: 70 percent / tBuOK / tetrahydrofuran
5.1: 73 percent / tBuOK / tetrahydrofuran
With
4-methyl-morpholine; TEA; potassium tert-butylate; hydrogen; isobutyl chloroformate;
palladium on activated charcoal; silver benzoate;
In
tetrahydrofuran; methanol;
2.1: Arndt-Eistert rearrangement;
DOI:10.1016/j.tetlet.2007.03.066
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: H2 / Pd/C / methanol
1.2: tetrahydrofuran
2.1: 70 percent / tBuOK / tetrahydrofuran
3.1: 73 percent / tBuOK / tetrahydrofuran
With
potassium tert-butylate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2007.03.066