(Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

Base Information

Chemical Name:(Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate
CAS No.:1428247-20-4
Molecular Formula:C₇H₈*C₃₂H₂₃NO₄Sn
Molecular Weight:696.389
Hs Code.:

(Ph<sub>3</sub>Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

Synonyms:(Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

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Chemical Property of (Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

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Technology Process of (Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

There total 2 articles about (Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 51411-04-2
alrestatin

: 76-87-9
triphenyltin(IV) hydroxide

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1428247-20-4
(Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

Guidance literature:: for 10h; Reflux; Dean-Stark;
DOI:10.1016/j.jorganchem.2013.01.017

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1428247-20-4
(Ph₃Sn)((1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-acetate) toluene solvate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 8 h / 90 °C

2: 10 h / Reflux; Dean-Stark

In N,N-dimethyl-formamide;
DOI:10.1016/j.jorganchem.2013.01.017