3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

Base Information

Chemical Name:3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide
CAS No.:934740-57-5
Molecular Formula:C₃₅H₃₈N₂O₃S
Molecular Weight:566.764
Hs Code.:

3-(4-<i>tert</i>-butoxy-phenyl)-<i>N</i>-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

Synonyms:3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

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Chemical Property of 3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

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Technology Process of 3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

There total 5 articles about 3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934740-49-5
[2-(4-tert-butoxy-phenyl)-1-methylcarbamoyl-ethyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

: 934740-57-5
3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: HCOONH₄ / Pd/C / methanol / 50 °C

2: 2.23 g / 1-hydroxybenzotriazole; HBTU; iPr₂NEt / dimethylformamide / 16 h / 20 °C

With ammonium formate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja0634573

Reference yield:

: 71989-38-3,118488-18-9,204384-67-8
Fmoc-Tyr(tBu)-OH

: 934740-57-5
3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-hydroxybenzotriazole; iPr₂NEt; HBTU / dimethylformamide / 0.17 h / 0 °C

1.2: 94 percent / dimethylformamide / 1.5 h / 20 °C

2.1: HCOONH₄ / Pd/C / methanol / 50 °C

3.1: 2.23 g / 1-hydroxybenzotriazole; HBTU; iPr₂NEt / dimethylformamide / 16 h / 20 °C

With ammonium formate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja0634573

Reference yield:

: 101363-71-7
2-amino-3-(4-tert-butoxy-phenyl)-N-methyl-propionamide

: 34914-36-8
2-(triphenylmethylthio)ethanoic acid

: 934740-57-5
3-(4-tert-butoxy-phenyl)-N-methyl-2-(2-tritylsulfanyl-acetylamino)-propionamide

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/ja0634573