diethyl 4,4'-bis(methoxycarboxylate)benzil

Base Information

Chemical Name:diethyl 4,4'-bis(methoxycarboxylate)benzil
CAS No.:229623-73-8
Molecular Formula:C₂₂H₂₂O₈
Molecular Weight:414.412
Hs Code.:

Synonyms:diethyl 4,4'-bis(methoxycarboxylate)benzil

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Chemical Property of diethyl 4,4'-bis(methoxycarboxylate)benzil

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Technology Process of diethyl 4,4'-bis(methoxycarboxylate)benzil

There total 2 articles about diethyl 4,4'-bis(methoxycarboxylate)benzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 105-36-2
ethyl bromoacetate

: 33288-79-8
4,4'-dihydroxybenzil

: 229623-73-8
diethyl 4,4'-bis(methoxycarboxylate)benzil

Guidance literature:: With potassium carbonate; In acetonitrile; for 24h; Heating;
DOI:10.1021/ol990536t

Reference yield:

: 1226-42-2
1,2-bis(4-methoxyphenyl)-1,2-ethanedione

: 229623-73-8
diethyl 4,4'-bis(methoxycarboxylate)benzil

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / pyridine*HCl / Heating

2: 80 percent / K₂CO₃ / acetonitrile / 24 h / Heating

With pyridine hydrochloride; potassium carbonate; In acetonitrile;
DOI:10.1021/ol990536t