methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

Base Information

Chemical Name:methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate
CAS No.:1262298-51-0
Molecular Formula:C₂₆H₃₂N₄O₃
Molecular Weight:448.565
Hs Code.:

Synonyms:methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

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Chemical Property of methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

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Technology Process of methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

There total 4 articles about methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262298-47-4
methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-methylbut-3-yn-2-yl)carbamate

: 622-37-7
Phenyl azide

: 1262298-51-0
methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

Guidance literature:: methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-methylbut-3-yn-2-yl)carbamate; Phenyl azide; With copper(II) sulphate hydrate; ascorbic acid; In water; tert-butyl alcohol; at 20 ℃; for 48h;

Phenyl azide; With copper(ll) sulfate pentahydrate; ascorbic acid; In water; tert-butyl alcohol; at 20 ℃; for 4h;

Reference yield:

: 936-59-4
3-chloropropiophenone

: 1262298-51-0
methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride; magnesium / hexane; tetrahydrofuran / 2 h / 20 - 30 °C / Inert atmosphere

1.2: 0.5 h / 0 °C / Inert atmosphere

1.3: 30 °C

2.1: potassium iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 80 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Cooling

3.2: 20 °C

4.1: ascorbic acid; copper(II) sulphate hydrate / water; tert-butyl alcohol / 48 h / 20 °C

4.2: 4 h / 20 °C

With copper(II) sulphate hydrate; diisobutylaluminium hydride; magnesium; N-ethyl-N,N-diisopropylamine; potassium iodide; ascorbic acid; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1110641-65-0
1-chloro-5-methyl-3-phenylhex-5-en-3-ol

: 1262298-51-0
methyl 3-hydroxy-5-methyl-3-phenylhex-5-enyl(2-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Cooling

2.2: 20 °C

3.1: ascorbic acid; copper(II) sulphate hydrate / water; tert-butyl alcohol / 48 h / 20 °C

3.2: 4 h / 20 °C

With copper(II) sulphate hydrate; N-ethyl-N,N-diisopropylamine; potassium iodide; ascorbic acid; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;