C₃₁H₃₁N₃O₈

Base Information

Chemical Name:C₃₁H₃₁N₃O₈
CAS No.:1276541-33-3
Molecular Formula:C₃₁H₃₁N₃O₈
Molecular Weight:573.602
Hs Code.:

C<sub>31</sub>H<sub>31</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₁H₃₁N₃O₈

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Chemical Property of C₃₁H₃₁N₃O₈

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Technology Process of C₃₁H₃₁N₃O₈

There total 4 articles about C₃₁H₃₁N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1276541-17-3
C₇H₇NO₃

: C₂₄H₂₆N₂O₅

: 1276541-33-3
C₃₁H₃₁N₃O₈

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at -78 - -50 ℃; for 3h;
DOI:10.1002/ejoc.201001629

Reference yield:

: 1276541-24-2
C₇H₉NO₃

: 1276541-33-3
C₃₁H₃₁N₃O₈

Guidance literature:: Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C

2: trifluorormethanesulfonic acid / dichloromethane / 3 h / -78 - -50 °C

With trifluorormethanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201001629

Reference yield:

: 2450-26-2
2-nitrovanillin

: 1276541-33-3
C₃₁H₃₁N₃O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / Reflux

1.2: 0.5 h / 20 °C

1.3: pH 6

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 4 h / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C

4.1: trifluorormethanesulfonic acid / dichloromethane / 3 h / -78 - -50 °C

With trifluorormethanesulfonic acid; palladium 10% on activated carbon; hydrogen; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201001629