2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

Base Information

Chemical Name:2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone
CAS No.:1384097-70-4
Molecular Formula:C₂₉H₃₀N₄O₆S
Molecular Weight:562.646
Hs Code.:

Synonyms:2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

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Chemical Property of 2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

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Technology Process of 2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

There total 5 articles about 2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1384097-71-5
(E)-4-(2,4-dimethoxybenzylideneamino)-3-(3,4,5-trimethoxyphenyl)-1H-1,2,4-triazole-5(4H)-thione

: 619-41-0
4-(bromoacetyl)toluene

: 1384097-70-4
2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

Guidance literature:: (E)-4-(2,4-dimethoxybenzylideneamino)-3-(3,4,5-trimethoxyphenyl)-1H-1,2,4-triazole-5(4H)-thione; With potassium carbonate; In acetone; for 0.5h; Reflux;

4-(bromoacetyl)toluene; In acetone; Reflux;
DOI:10.1016/j.bmcl.2012.03.023

Reference yield:

: 118-41-2
Eudesmic acid

: 1384097-70-4
2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 12 h / Reflux

2.1: hydrazine hydrate / ethanol / 6 h / Reflux

3.1: potassium hydroxide / ethanol / 16 h / 20 °C

3.2: 3 h / Reflux

4.1: acetic acid / 2 h / Reflux

5.1: potassium carbonate / acetone / 0.5 h / Reflux

5.2: Reflux

With sulfuric acid; potassium carbonate; hydrazine hydrate; acetic acid; potassium hydroxide; In ethanol; acetone;
DOI:10.1016/j.bmcl.2012.03.023

Reference yield:

: 31821-78-0
4-amino-3-(3,4,5-trimethoxyphenyl)-1H-1,2,4-triazole-5(4H)-thione

: 1384097-70-4
2-(6-(2,4-dimethoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-5,6-dihydro-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl)-1-p-tolylethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 2 h / Reflux

2.1: potassium carbonate / acetone / 0.5 h / Reflux

2.2: Reflux

With potassium carbonate; acetic acid; In acetone;
DOI:10.1016/j.bmcl.2012.03.023