(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

Base Information

Chemical Name:(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol
CAS No.:1198463-48-7
Molecular Formula:C₂₅H₃₆O₆
Molecular Weight:432.557
Hs Code.:

Synonyms:(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

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Chemical Property of (3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

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Technology Process of (3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

There total 1 articles about (3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1198463-64-7
C₂₅H₃₄O₆

: 1198463-48-7
(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

: 1198463-65-8
(3S,4S,6R,E)-4-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -35 - 0 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja907924j

Reference yield: 99.0%

: 1198463-48-7
(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

: 209065-57-6
2-[bis(2,2,2-trifluoroethoxy)phosphoryl]acetic acid

: 1198463-38-5
(3S,4S,6R,1E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(2S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-yl 2-[bis(2,2,2-trifluoroethoxy)phosphoryl]acetate

Guidance literature:: (3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol; 2-[bis(2,2,2-trifluoroethoxy)phosphoryl]acetic acid; With 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

With dmap; In benzene; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja907924j

Reference yield: 18.0%

: 1198463-48-7
(3S,4S,6R,E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-ol

: 1379586-79-4
4-((2R,6R)-6-((S)-2-methylpent-4-ynyl)-5,6-dihydro-2H-pyran-2-yl)but-2-ynoic acid

: 1379586-80-7
(3S,4S,6R,1E)-3-(4-methoxybenzyloxy)-6-(methoxymethoxy)-1-[(2S)-4-methyl-3,6-dihydro-2H-pyran-2-yl]nona-1,8-dien-4-yl 4-{(2R,6R)-6-[(2S)-2-methylpent-4-ynyl]-5,6-dihydro-2H-pyran-2-yl}but-2-ynoate

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/chem.201102899