1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

Base Information

Chemical Name:1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene
CAS No.:906098-32-6
Molecular Formula:C₃₅H₃₅ClO₃
Molecular Weight:539.114
Hs Code.:

Synonyms:1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

Chemical Property:

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Technology Process of 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

There total 10 articles about 1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₄₀ClNO₅Se

: 906098-32-6
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo0607562

Reference yield:

: 906098-29-1
(3S,4R,5R,6S)-3-(4-chlorophenyl)-4,5,6-tri(benzyloxy)-7-octen-1-ol

: 906098-32-6
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₃P / tetrahydrofuran

2: aq. H₂O₂ / tetrahydrofuran / 20 °C

With tributylphosphine; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/jo0607562

Reference yield:

: 906098-26-8
methyl (3S,4R,5R,6S)-3-(4-chlorophenyl)-4,5,6-tri(benzyloxy)-7-octenoate

: 906098-32-6
1-((3S,4R,5R,6S)-4,5,6-tri(benzyloxy)octa-1,7-dien-3-yl)-4-chlorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 3 h / 0 - 20 °C

2: Bu₃P / tetrahydrofuran

3: aq. H₂O₂ / tetrahydrofuran / 20 °C

With lithium aluminium tetrahydride; tributylphosphine; dihydrogen peroxide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo0607562