bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

Base Information

Chemical Name:bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide
CAS No.:630426-42-5
Molecular Formula:C₅₂H₇₀O₄S₃
Molecular Weight:855.323
Hs Code.:

Synonyms:bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

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Technology Process of bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

There total 5 articles about bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 251291-83-5
(E,E)-bis(4-chloro-3-methyl-2-butenyl) sulfide

: 356793-88-9
3,7,11-trimethyl-1-(phenylsulfonyl)dodeca-2,4,6,10-tetraene

: 630426-42-5
bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

Guidance literature:: With sodium hydride; sodium iodide; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1002/hlca.200390211

Reference yield:

: 56691-80-6
geranyl phenyl sulfone

: 630426-42-5
bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / BuLi / tetrahydrofuran; hexane / 0 - 20 °C

2: 75 percent / NaOEt / ethanol / 10 h / Heating

3: 55 percent / LiNbMoO₆; H₂O₂ / methanol; benzene; H₂O / 6 h / 20 °C

4: 90 percent / NaH; NaI / tetrahydrofuran / 15 h / 20 °C

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; sodium ethanolate; sodium hydride; sodium iodide; In tetrahydrofuran; methanol; ethanol; hexane; water; benzene;
DOI:10.1002/hlca.200390211

Reference yield:

: 3,7,11-trimethyl-1-(phenylsulfanyl)dodeca-2,4,6,10-tetraene

: 630426-42-5
bis[3,7,11,15-tetramethyl-5-(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaenyl] sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / LiNbMoO₆; H₂O₂ / methanol; benzene; H₂O / 6 h / 20 °C

2: 90 percent / NaH; NaI / tetrahydrofuran / 15 h / 20 °C

With LiNbMoO₆; dihydrogen peroxide; sodium hydride; sodium iodide; In tetrahydrofuran; methanol; water; benzene;
DOI:10.1002/hlca.200390211